Non-stoichiometry and twinning in NbN1-x: A study of synthesis and structure in a defect NaCl-type solid

S. J. Kim; H. F. Franzen; W. Lengauer

doi:10.1016/0022-5088(90)90122-Z

Non-stoichiometry and twinning in NbN_1-x: A study of synthesis and structure in a defect NaCl-type solid

S. J. Kim, H. F. Franzen, W. Lengauer

Department of Chemistry & Nanoscience

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

Samples of high-purity NbN_1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN_1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN_1-x.

Original language	English
Pages (from-to)	193-196
Number of pages	4
Journal	Journal of The Less-Common Metals
Volume	160
Issue number	1
DOIs	https://doi.org/10.1016/0022-5088(90)90122-Z
State	Published - 15 Apr 1990

Bibliographical note

Funding Information:
The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.

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10.1016/0022-5088(90)90122-Z

Cite this

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abstract = "Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.",

author = "Kim, {S. J.} and Franzen, {H. F.} and W. Lengauer",

note = "Funding Information: The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.",

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T2 - A study of synthesis and structure in a defect NaCl-type solid

AU - Kim, S. J.

AU - Franzen, H. F.

AU - Lengauer, W.

N1 - Funding Information: The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.

PY - 1990/4/15

Y1 - 1990/4/15

N2 - Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.

AB - Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.

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