Non-stoichiometry and twinning in NbN1-x: A study of synthesis and structure in a defect NaCl-type solid

S. J. Kim; H. F. Franzen; W. Lengauer

doi:10.1016/0022-5088(90)90122-Z

Non-stoichiometry and twinning in NbN_1-x: A study of synthesis and structure in a defect NaCl-type solid

S. J. Kim, H. F. Franzen, W. Lengauer

Department of Chemistry & Nanoscience

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

Samples of high-purity NbN_1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN_1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN_1-x.

Original language	English
Pages (from-to)	193-196
Number of pages	4
Journal	Journal of The Less-Common Metals
Volume	160
Issue number	1
DOIs	https://doi.org/10.1016/0022-5088(90)90122-Z
State	Published - 15 Apr 1990

Bibliographical note

Funding Information:
The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.

Access to Document

10.1016/0022-5088(90)90122-Z

Cite this

@article{47b295a570e0482e98839a309dd6edb0,

title = "Non-stoichiometry and twinning in NbN1-x: A study of synthesis and structure in a defect NaCl-type solid",

abstract = "Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.",

author = "Kim, {S. J.} and Franzen, {H. F.} and W. Lengauer",

note = "Funding Information: The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.",

year = "1990",

month = apr,

day = "15",

doi = "10.1016/0022-5088(90)90122-Z",

language = "English",

volume = "160",

pages = "193--196",

journal = "Journal of The Less-Common Metals",

issn = "0022-5088",

publisher = "Elsevier BV",

number = "1",

}

TY - JOUR

T1 - Non-stoichiometry and twinning in NbN1-x

T2 - A study of synthesis and structure in a defect NaCl-type solid

AU - Kim, S. J.

AU - Franzen, H. F.

AU - Lengauer, W.

N1 - Funding Information: The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.

PY - 1990/4/15

Y1 - 1990/4/15

N2 - Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.

AB - Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.

UR - http://www.scopus.com/inward/record.url?scp=0025417629&partnerID=8YFLogxK

U2 - 10.1016/0022-5088(90)90122-Z

DO - 10.1016/0022-5088(90)90122-Z

M3 - Article

AN - SCOPUS:0025417629

SN - 0022-5088

VL - 160

SP - 193

EP - 196

JO - Journal of The Less-Common Metals

JF - Journal of The Less-Common Metals

IS - 1