Non-stoichiometry and twinning in NbN1-x: A study of synthesis and structure in a defect NaCl-type solid

S. J. Kim, H. F. Franzen, W. Lengauer

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Abstract

Samples of high-purity NbN1-x were prepared by a high temperature technique. Single-crystal studies revealed the twinning of the tetragonal low temperature phase which forms when cubic NbN1-x is cooled from a high temperature. The X-ray diffraction results confirm the previously found structure of tetragonal NbN1-x.

Original languageEnglish
Pages (from-to)193-196
Number of pages4
JournalJournal of The Less-Common Metals
Volume160
Issue number1
DOIs
StatePublished - 15 Apr 1990

Bibliographical note

Funding Information:
The Ames Laboratory-DOE is operatedf or the U.S. Departmento f Energy by Iowa StateU niversity under Contract No. W-7405-Eng-82. This researchw as supportedb y the Office of Basic Energy Sciences,M aterialsS ciencesD ivision.

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