Morphology controlled synthesis of nanostructured Bi2Te 3

Hee Jin Kim; Mi Kyung Han; Ha Young Kim; Wooyoung Lee; Sung Jin Kim

doi:10.5012/bkcs.2012.33.12.3977

Morphology controlled synthesis of nanostructured Bi₂Te ₃

Hee Jin Kim, Mi Kyung Han, Ha Young Kim, Wooyoung Lee, Sung Jin Kim

Department of Chemistry & Nanoscience

Research output: Contribution to journal › Article › peer-review

19 Scopus citations

Abstract

Nanostructured thermoelectric bismuth telluride (Bi₂Te ₃) powders with various morphologies, such as nanoplates, nanorods, and nanotubes, were prepared by a hydrothermal method based on the reaction between BiCl₃, Te, and sodium ethylenediaminetetraacetate (Na ₂-EDTA) at 150, 180, and 210 °C. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and selected area electron diffraction (SAED). The effect of reaction temperature on the morphology of the Bi₂Te₃ particles was investigated, and the possible mechanism of morphology control was proposed.

Original language	English
Pages (from-to)	3977-3980
Number of pages	4
Journal	Bulletin of the Korean Chemical Society
Volume	33
Issue number	12
DOIs	https://doi.org/10.5012/bkcs.2012.33.12.3977
State	Published - 20 Dec 2012

Keywords

BiTe
Growth mechanism
Nanoparticle
Nanorod
Thermoelectric material

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10.5012/bkcs.2012.33.12.3977

Cite this

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title = "Morphology controlled synthesis of nanostructured Bi2Te 3",

abstract = "Nanostructured thermoelectric bismuth telluride (Bi2Te 3) powders with various morphologies, such as nanoplates, nanorods, and nanotubes, were prepared by a hydrothermal method based on the reaction between BiCl3, Te, and sodium ethylenediaminetetraacetate (Na 2-EDTA) at 150, 180, and 210 °C. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and selected area electron diffraction (SAED). The effect of reaction temperature on the morphology of the Bi2Te3 particles was investigated, and the possible mechanism of morphology control was proposed.",

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author = "Kim, \{Hee Jin\} and Han, \{Mi Kyung\} and Kim, \{Ha Young\} and Wooyoung Lee and Kim, \{Sung Jin\}",

year = "2012",

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doi = "10.5012/bkcs.2012.33.12.3977",

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TY - JOUR

T1 - Morphology controlled synthesis of nanostructured Bi2Te 3

AU - Kim, Hee Jin

AU - Han, Mi Kyung

AU - Kim, Ha Young

AU - Lee, Wooyoung

AU - Kim, Sung Jin

PY - 2012/12/20

Y1 - 2012/12/20

N2 - Nanostructured thermoelectric bismuth telluride (Bi2Te 3) powders with various morphologies, such as nanoplates, nanorods, and nanotubes, were prepared by a hydrothermal method based on the reaction between BiCl3, Te, and sodium ethylenediaminetetraacetate (Na 2-EDTA) at 150, 180, and 210 °C. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and selected area electron diffraction (SAED). The effect of reaction temperature on the morphology of the Bi2Te3 particles was investigated, and the possible mechanism of morphology control was proposed.

AB - Nanostructured thermoelectric bismuth telluride (Bi2Te 3) powders with various morphologies, such as nanoplates, nanorods, and nanotubes, were prepared by a hydrothermal method based on the reaction between BiCl3, Te, and sodium ethylenediaminetetraacetate (Na 2-EDTA) at 150, 180, and 210 °C. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and selected area electron diffraction (SAED). The effect of reaction temperature on the morphology of the Bi2Te3 particles was investigated, and the possible mechanism of morphology control was proposed.

KW - BiTe

KW - Growth mechanism

KW - Nanoparticle

KW - Nanorod

KW - Thermoelectric material

UR - https://www.scopus.com/pages/publications/84871743778

U2 - 10.5012/bkcs.2012.33.12.3977

DO - 10.5012/bkcs.2012.33.12.3977

M3 - Article

AN - SCOPUS:84871743778

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VL - 33

SP - 3977

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JO - Bulletin of the Korean Chemical Society

JF - Bulletin of the Korean Chemical Society

IS - 12