Curing behaviors of transparent aliphatic epoxy acrylate by electron beam irradiation

Sang Yul Park; Hyemi Son; Dongshin Myung; Myung Hwa Kim; Young Soo Seo

doi:10.7317/pk.2013.37.3.302

Curing behaviors of transparent aliphatic epoxy acrylate by electron beam irradiation

Sang Yul Park, Hyemi Son, Dongshin Myung, Myung Hwa Kim, Young Soo Seo

Department of Chemistry & Nanoscience

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

We synthesized aliphatic epoxy acrylate monomer by the reaction of glycerol diglycidyl ether and acrylic acid. The reaction was monitored by FTIR, Raman spectroscopy and ¹H NMR. Electron-beam (E-beam) curing behaviors of the synthesized monomer were studied by spectroscopic analysis, glass transition temperature, and tensile properties. We found that curing reaction was complete in a low dosage of ca. 30 kGy. The viscosity of monomer was a low enough for coating without using diluents and the cured sample was highly transparent, indicating that the monomer can be used for an E-beam curable coating material on transparent optical films.

Original language	English
Pages (from-to)	302-307
Number of pages	6
Journal	Polymer (Korea)
Volume	37
Issue number	3
DOIs	https://doi.org/10.7317/pk.2013.37.3.302
State	Published - May 2013

Keywords

Aliphatic epoxy acrylate
Electron beam curing
FTIR
Raman spectroscopy
Transparent optical films

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title = "Curing behaviors of transparent aliphatic epoxy acrylate by electron beam irradiation",

abstract = "We synthesized aliphatic epoxy acrylate monomer by the reaction of glycerol diglycidyl ether and acrylic acid. The reaction was monitored by FTIR, Raman spectroscopy and 1H NMR. Electron-beam (E-beam) curing behaviors of the synthesized monomer were studied by spectroscopic analysis, glass transition temperature, and tensile properties. We found that curing reaction was complete in a low dosage of ca. 30 kGy. The viscosity of monomer was a low enough for coating without using diluents and the cured sample was highly transparent, indicating that the monomer can be used for an E-beam curable coating material on transparent optical films.",

keywords = "Aliphatic epoxy acrylate, Electron beam curing, FTIR, Raman spectroscopy, Transparent optical films",

author = "Park, {Sang Yul} and Hyemi Son and Dongshin Myung and Kim, {Myung Hwa} and Seo, {Young Soo}",

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T1 - Curing behaviors of transparent aliphatic epoxy acrylate by electron beam irradiation

AU - Park, Sang Yul

AU - Son, Hyemi

AU - Myung, Dongshin

AU - Kim, Myung Hwa

AU - Seo, Young Soo

PY - 2013/5

Y1 - 2013/5

N2 - We synthesized aliphatic epoxy acrylate monomer by the reaction of glycerol diglycidyl ether and acrylic acid. The reaction was monitored by FTIR, Raman spectroscopy and 1H NMR. Electron-beam (E-beam) curing behaviors of the synthesized monomer were studied by spectroscopic analysis, glass transition temperature, and tensile properties. We found that curing reaction was complete in a low dosage of ca. 30 kGy. The viscosity of monomer was a low enough for coating without using diluents and the cured sample was highly transparent, indicating that the monomer can be used for an E-beam curable coating material on transparent optical films.

AB - We synthesized aliphatic epoxy acrylate monomer by the reaction of glycerol diglycidyl ether and acrylic acid. The reaction was monitored by FTIR, Raman spectroscopy and 1H NMR. Electron-beam (E-beam) curing behaviors of the synthesized monomer were studied by spectroscopic analysis, glass transition temperature, and tensile properties. We found that curing reaction was complete in a low dosage of ca. 30 kGy. The viscosity of monomer was a low enough for coating without using diluents and the cured sample was highly transparent, indicating that the monomer can be used for an E-beam curable coating material on transparent optical films.

KW - Aliphatic epoxy acrylate

KW - Electron beam curing

KW - FTIR

KW - Raman spectroscopy

KW - Transparent optical films

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SN - 0379-153X

VL - 37

SP - 302

EP - 307

JO - Polymer (Korea)

JF - Polymer (Korea)

IS - 3

ER -

Curing behaviors of transparent aliphatic epoxy acrylate by electron beam irradiation

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Keywords

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